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Crystallization

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Supaphol P, Spruiell JE (2000) Thermal properties and isothermal crystallization of syndiotactic polypropylenes: Differential scanning calorimetry and overall crystallization kinetics. J Appl Polym Sci 75(1):44–59. https://doi.org/10.1002/(sici)1097-4628(20000103)75:1%3c44:Aid-app6%3e3.0.Co;2-1 Okada T, Saito H, Inoue T (1992) Time resolved light scattering studies on the early stages of crystallization in isotactic polypropylene. Macromolecules 25:1908–1911 Schultz JM (1984) Microstructural aspects of failure in semicrystalline polymers. Polym Eng Sci 24(10):770–785. https://doi.org/10.1002/pen.760241007 Varga J, Ehrenstein GW (1997) High-temperature hedritic crystallization of the beta-modification of isotactic polypropylene. Colloid Polym Sci 275(6):511–519. https://doi.org/10.1007/s003960050113 Keith HD, Padden FJ (1963) A phenomenological theory of spherulitic crystallization. J Appl Phys 34(8):2409–2421. https://doi.org/10.1063/1.1702757

Lauritzen JI, Hoffman JD (1973) Extension of theory of growth of chain-folded polymer crystals to large undercoolings. J Appl Phys 44(10):4340–4352. https://doi.org/10.1063/1.1661962 By using this service, you agree that you will only keep content for personal use, and will not openly distribute them via Dropbox, Google Drive or other file sharing services Lotz B, Lovinger AJ, Cais RE (1988) Crystal-structure and morphology of syndiotactic polypropylene single-crystals. Macromolecules 21(8):2375–2382. https://doi.org/10.1021/ma00186a013 Kaminsky W (1998) Highly active metallocene catalysts for olefin polymerization. J Chem Soc, Dalton Trans 9:1413–1418. https://doi.org/10.1039/A800056E Hoffman JD, Davis GT, Lauritzen JI (1976) Crystalline and noncrystalline solids. In: Hannay NB (ed) Treatise on solid state chemistry, vol 3. Plenum, New YorkPetermann J, Gohil RM, Schultz JM et al (1982) The kinetics of defect clustering in fibrillar polypropylene crystals. J Polym Sci Part B Polym Phys 20(3):523–534. https://doi.org/10.1002/pol.1982.180200313 Kinetic Characterization of Precipitation Reactions: Possible Link between a Phenomenological Equation and Reaction Pathway. Suetsugu Y, Kikutani T, Kyu T et al (1990) An experimental technique for characterizing dispersion in compounds of particulates in thermoplastics using small-angle light scattering. Colloid Polym Sci 268(2):118–131. https://doi.org/10.1007/bf01513190 The fixed number of water molecules contained in one formula unit of a salt is known as water of crystallisation. Or, to put it another way, water that is stoichiometrically bonded into crystal. CuSO 4 5H 2O is the chemical formula for hydrated copper sulphate, for example. Copper sulphate crystallises with 5 molecules of water. Janeschitz-Kriegl H, Ratajski E, Stadlbauer M (2003) Flow as an effective promotor of nucleation in polymer melts: a quantitative evaluation. Rheol Acta 42(4):355–364. https://doi.org/10.1007/s00397-002-0247-x

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Incorporating all the recent developments and applications of crystallization technology, Crystallization gives clear accounts of the underlying principles, a review of the past and current research themes and guidelines for equipment and process design. This new edition introduces and enlarges upon such subjects as: Morrow DR, Sauer JA, Woodward AE (1965) Dilute solution-grown polypropylene single crystals. J Polym Sci Part B Polym Lett 3(6):463–466. https://doi.org/10.1002/pol.1965.110030608

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Turnbull D, Fisher JC (1949) Rate of nucleation in condensed systems. J Chem Phys 17(1):71–73. https://doi.org/10.1063/1.1747055 Rodriguez-Arnold J, Zhang AQ, Cheng SZD et al (1994) Crystallization, melting and morphology of syndiotactic polypropylene fractions. 1. Thermodynamic properties, overall crystallization and melting. Polymer 35(9):1884–1895. https://doi.org/10.1016/0032-3861(94)90978-4 Wang X, Hou WM, Zhou JJ et al (2007) Melting behavior of lamellae of isotactic polypropylene studied using hot-stage atomic force microscopy. Colloid Polym Sci 285(4):449–455. https://doi.org/10.1007/s00396-006-1586-4 De Rosa C, Auriemma F (2006) Structure and physical properties of syndiotactic polypropylene: a highly crystalline thermoplastic elastomer. Prog Polym Sci 31(2):145–237. https://doi.org/10.1016/j.progpolymsci.2005.11.002

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